C₂₅H₃₁N₃O₆

Base Information

Chemical Name:C₂₅H₃₁N₃O₆
CAS No.:1351707-85-1
Molecular Formula:C₂₅H₃₁N₃O₆
Molecular Weight:469.538
Hs Code.:

C<sub>25</sub>H<sub>31</sub>N<sub>3</sub>O<sub>6</sub>

Synonyms:C₂₅H₃₁N₃O₆

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Chemical Property of C₂₅H₃₁N₃O₆

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Technology Process of C₂₅H₃₁N₃O₆

There total 3 articles about C₂₅H₃₁N₃O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 111474-74-9
3-(4-methoxyphenyl)indolin-2-one

: 1351707-85-1
C₂₅H₃₁N₃O₆

Guidance literature:: 3-(4-methoxyphenyl)indolin-2-one; With C₃₀H₃₀F₆N₄OS; In tetrahydrofuran; at -10 ℃; for 0.5h; Inert atmosphere;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; at -10 ℃; for 120h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/adsc.201100379

Reference yield:

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 111474-74-9
3-(4-methoxyphenyl)indolin-2-one

: 1351707-85-1
C₂₅H₃₁N₃O₆

: C₂₅H₃₁N₃O₆

Guidance literature:: With cinchonidine derived-catalyst; In 1,2-dichloro-ethane; at 0 ℃; for 48h; Molecular sieve;
DOI:10.1039/c5cc10096h

Reference yield:

: 3265-29-0
3-diazo-indolin-2-one

: 100-66-3
methoxybenzene

: 1351707-85-1
C₂₅H₃₁N₃O₆

: C₂₅H₃₁N₃O₆

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoromethanesulfonyloxy(triphenylphosphine)gold(I) / dichloromethane / 5 h / -10 °C / Inert atmosphere; Schlenk technique

2: cinchonidine derived-catalyst / 1,2-dichloro-ethane / 48 h / 0 °C / Molecular sieve

With trifluoromethanesulfonyloxy(triphenylphosphine)gold(I); In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/c5cc10096h