C₈H₁₀N₂O₂

Base Information

Chemical Name:C₈H₁₀N₂O₂
CAS No.:1256554-06-9
Molecular Formula:C₈H₁₀N₂O₂
Molecular Weight:166.18
Hs Code.:

C<sub>8</sub>H<sub>10</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₈H₁₀N₂O₂

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Chemical Property of C₈H₁₀N₂O₂

Chemical Property:

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Technology Process of C₈H₁₀N₂O₂

There total 5 articles about C₈H₁₀N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354724-03-0
C₁₅H₁₆N₂O₃

: 1256554-06-9
C₈H₁₀N₂O₂

Guidance literature:: With ammonium cerium (IV) nitrate; water; In acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1002/chem.201201192

Reference yield:

: 100-52-7
benzaldehyde

: 1256554-06-9
C₈H₁₀N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium acetate / ethanol / 24 h / 20 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux; Inert atmosphere

3: titanium tetrachloride; triethylamine / toluene / 12 h / 0 - 20 °C / Inert atmosphere

4: (R)-N-(phenylcarbamoyl)-tert-butanesulfinamide; trichlorosilane; water / acetonitrile / 24 h / -40 °C

5: ammonium cerium (IV) nitrate; water / acetonitrile / 0.5 h / 0 °C

With ammonium cerium (IV) nitrate; (R)-N-(phenylcarbamoyl)-tert-butanesulfinamide; trichlorosilane; water; sodium acetate; titanium tetrachloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; ethyl acetate; toluene; acetonitrile;
DOI:10.1002/chem.201201192

Reference yield:

: 141377-54-0,145920-96-3,149495-00-1,15990-45-1
2-nitro-1-phenylethan-1-ol

: 1256554-06-9
C₈H₁₀N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux; Inert atmosphere

2: titanium tetrachloride; triethylamine / toluene / 12 h / 0 - 20 °C / Inert atmosphere

3: (R)-N-(phenylcarbamoyl)-tert-butanesulfinamide; trichlorosilane; water / acetonitrile / 24 h / -40 °C

4: ammonium cerium (IV) nitrate; water / acetonitrile / 0.5 h / 0 °C

With ammonium cerium (IV) nitrate; (R)-N-(phenylcarbamoyl)-tert-butanesulfinamide; trichlorosilane; water; titanium tetrachloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethyl acetate; toluene; acetonitrile;
DOI:10.1002/chem.201201192