N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine

Base Information

Chemical Name:N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine
CAS No.:55577-67-8
Molecular Formula:C₁₅H₁₄N₂O₃
Molecular Weight:270.288
Hs Code.:
NSC Number:518112
DSSTox Substance ID:DTXSID10419745
Nikkaji Number:J3.102.013A

Synonyms:NSC518112;55577-67-8;DTXSID10419745;NSC-518112;N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine

Suppliers and Price of N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine

Chemical Property:

Vapor Pressure:2.54E-07mmHg at 25°C
Boiling Point:421.8°Cat760mmHg
Flash Point:208.9°C
Density:1.24g/cm³
XLogP3:4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:270.10044231
Heavy Atom Count:20
Complexity:338

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)NC(=C[N+](=O)[O-])C2=CC=CC=C2
Isomeric SMILES:COC1=CC=C(C=C1)N/C(=C/[N+](=O)[O-])/C2=CC=CC=C2

Technology Process of N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine

There total 7 articles about N-(4-Methoxyphenyl)-1-phenyl-2-nitroethene-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 104-94-9
4-methoxy-aniline

: 614-21-1
2-nitroacetophenone

: 55577-67-8
(Z)-4-methoxy-N-(2-nitro-1-phenylvinyl)aniline

Guidance literature:: With acetic acid; at 80 ℃; for 6h; Inert atmosphere;
DOI:10.1039/d1ob01453f

Reference yield: 20.0%

: 104-94-9
4-methoxy-aniline

: 614-21-1
2-nitroacetophenone

: 55577-67-8
(4-Methoxy-phenyl)-((E)-2-nitro-1-phenyl-vinyl)-amine

Guidance literature:: With titanium tetrachloride; triethylamine; In toluene; at 0 - 70 ℃; for 18h;
DOI:10.1055/s-0036-1591911

Reference yield:

: 100-52-7
benzaldehyde

: 55577-67-8
(4-Methoxy-phenyl)-((E)-2-nitro-1-phenyl-vinyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate / ethanol / 24 h / 20 °C / Inert atmosphere

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux; Inert atmosphere

3: titanium tetrachloride; triethylamine / toluene / 12 h / 0 - 20 °C / Inert atmosphere

With sodium acetate; titanium tetrachloride; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In ethanol; ethyl acetate; toluene;
DOI:10.1002/chem.201201192