(R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide

Base Information

• Chemical Name: (R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide
• CAS No.: 69555-88-0
• Molecular Formula: BrH*C₁₅H₁₄N₂O₄
• Molecular Weight: 367.199

Synonyms:(R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide

Chemical Property of (R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide

Chemical Property:

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Technology Process of (R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide

There total 1 articles about (R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrophenyl N-(benzyloxycarbonyl)-D-phenylalaninate (2578-85-0) → (R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide (69555-88-0)

Guidance literature:

With hydrogen bromide;

DOI:10.1021/jo00116a016

Reference yield:

(R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide (69555-88-0) + (+)-(7R,8S)-1,14-dimethoxy-7,8-bis(mercaptomethyl)-3,6,9,12-tetraoxatetradecane (104128-59-8) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + (R)-2-Amino-3-phenyl-thiopropionic acid S-{(2R,3R)-4-mercapto-2,3-bis-[2-(2-methoxy-ethoxy)-ethoxy]-butyl} ester; hydrobromide

Guidance literature:

In ethanol; dichloromethane; at 25 ℃; Rate constant; pH=5.4;

Reference yield:

(R)-2-Amino-3-phenyl-propionic acid 4-nitro-phenyl ester; hydrobromide (69555-88-0) + (2R,3S)-2-mercaptomethyl-3-methyl-1,4,7,10,13,16-hexaoxacyclooctadecane (104128-57-6) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + (R)-2-Amino-3-phenyl-thiopropionic acid S-((2R,3S)-3-methyl-1,4,7,10,13,16-hexaoxa-cyclooctadec-2-ylmethyl) ester; hydrobromide

Guidance literature:

In ethanol; dichloromethane; at 25 ℃; Rate constant; pH=5.4;

upstream raw materials:

p-nitrophenyl N-(benzyloxycarbonyl)-D-phenylalaninate

Downstream raw materials:

4-nitro-phenol

p-nitrophenyl N-dodecanoyl-D-phenylalaninate

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