N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

Base Information

Chemical Name:N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine
CAS No.:1162643-37-9
Molecular Formula:C₂₇H₄₄N₄O₂Si₂
Molecular Weight:512.843
Hs Code.:

Synonyms:N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

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Technology Process of N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

There total 1 articles about N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 74489-49-9
4-azidobenzyl bromide

: 165749-18-8
2-(3,4-bis((tert-butyldimethylsilyl)oxy)phenyl)ethan-1-amine

: 1162643-37-9
N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; caesium carbonate; In chloroform; acetonitrile; at 20 ℃; for 1.5h;
DOI:10.1016/j.bmc.2009.03.031

Reference yield: 76.0%

: 1162643-37-9
N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

: 1162643-42-6
2-methylquinoline-8-[p-(N'-2-propylureido)benzenesulfonyloxy]-5-{N,N'-dimethyl-N'-[2-(D-biotinylamino)ethyl]}sulfonamide

: 1162643-43-7
1-(4-{2-[3,4-bis(tert-butylsilyloxy)phenyl]ethylaminomethyl}phenyl)-4-{2-methylquinoline-8-[p-(N'-2-propynylureido)benzensulfonyloxy]}-5-{N,N'-dimethyl-N-[2-(D-biotinylamino)]sulfamoyl}-1,2,3-triazole

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 20 ℃; for 29h;
DOI:10.1016/j.bmc.2009.03.031

Reference yield: 63.0%

: 1162643-37-9
N-(4-azidobenzyl)-N-(2-[3,4-bis(tert-butyldimethylsilyloxy)phenyl]ethyl)amine

: C₄₄H₆₀N₈O₁₁S₃

: C₇₁H₁₀₄N₁₂O₁₃S₃Si₂

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.3987/COM-10-S(E)124