<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

Base Information

Chemical Name:<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol
CAS No.:149091-77-0
Molecular Formula:C₁₉H₂₉NO₈
Molecular Weight:399.441
Hs Code.:

Synonyms:<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

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Chemical Property of <1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

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Technology Process of <1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

There total 2 articles about <1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149091-76-9
<1R-(1α,2β,3α,4β,5β)>-5-Azido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

: 149091-77-0
<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 2 h / Ambient temperature

2: methanol / 5 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1016/S0040-4039(00)60330-1 DOI:10.1021/jo00083a023

Reference yield:

: 108-24-7
acetic anhydride

: 160799-84-8
(1R,2R,3S,4R,5S)-2-Amino-5-benzyloxy-1-hydroxymethyl-3,4-bis-methoxymethoxy-cyclopentanol

: 149091-77-0
<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

Guidance literature:: In methanol; for 5h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)60330-1 DOI:10.1021/jo00083a023

Reference yield:

: 149091-77-0
<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-2-(benzyloxy)-1-(hydroxymethyl)-3,4-bis(methoxymethoxy)-1-cyclopentanol

: 154540-30-4
<1R-(1α,2β,3α,4β,5β)>-5-Acetamido-1,3,4-triacetoxy-1-(acetoxymethyl)-2-(benzyloxy)cyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 10percent HCl / methanol / 1.) r.t., 5 min, 2.) 50 deg C, 20 min

2: DMAP, pyridine / 24 h / Ambient temperature

With pyridine; hydrogenchloride; dmap; In methanol;
DOI:10.1021/jo00083a023