Dipp₂nacnacAlCl₂

Base Information

• Chemical Name: Dipp₂nacnacAlCl₂
• CAS No.: 349545-04-6
• Molecular Formula: C₂₉H₄₁AlCl₂N₂
• Molecular Weight: 515.545

Synonyms:Dipp₂nacnacAlCl₂

Chemical Property of Dipp₂nacnacAlCl₂

Chemical Property:

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Technology Process of Dipp₂nacnacAlCl₂

There total 2 articles about Dipp₂nacnacAlCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene → Dipp2nacnacAlCl2 (349545-04-6)

Guidance literature:

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene; With n-butyllithium; In cyclohexane; toluene; at 0 - 20 ℃; for 1h;

With aluminum (III) chloride; In cyclohexane; toluene; at 20 ℃;

DOI:10.1002/chem.201502205

Reference yield: 73.0%

aluminium trichloride (7446-70-0) + Dipp2nacnacLi*Et2O (334719-92-5,872515-36-1) → Dipp2nacnacAlCl2 (349545-04-6)

Guidance literature:

In toluene; byproducts: LiCl; toluene soln. of ligand was added dropwise to AlCl3 at 0°C with stirring under inert atm., warmed to room temp. overnight; solvent was removed under reduced pressure, extd. with hexane, filtered,concd., cooled; elem. anal.;

DOI:10.1021/ic001311d

Reference yield: 90.0%

3,3-Dimethylbut-1-yne (917-92-0) + Dipp2nacnacAlCl2 (349545-04-6) → C41H59AlN2

Guidance literature:

3,3-Dimethylbut-1-yne; With n-butyllithium; In hexane; toluene; at -20 - 20 ℃; for 10h; Inert atmosphere; Schlenk technique; Glovebox;

Dipp₂nacnacAlCl₂; In hexane; toluene; at -20 ℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Reflux;

DOI:10.1002/anie.202000899

upstream raw materials:

aluminium trichloride

Dipp₂nacnacLi*Et₂O

Downstream raw materials:

(HC[(CMe)(N-2,6-iPr₂C₆H₃)]2)Al(OH)2

[(CH(C(CH₃)N(C₆H₃(CH(CH₃)2)2))2)Al(NH₂)2]

HC[C(Me)N(2,6-iPr₂C₆H₃)]2Al(Cl)NMe₂

(((CH₃)2CH)2C₆H₃NC(CH₃)CHC(CH₃)NC₆H₃(CH(CH₃)2)2)AlCl(OC₂H₅)

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