(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

Base Information

Chemical Name:(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄
CAS No.:608517-37-9
Molecular Formula:C₅₆H₅₄N₄O₂
Molecular Weight:815.07
Hs Code.:

(CH<sub>3</sub>OC<sub>6</sub>H<sub>3</sub>C<sub>5</sub>H<sub>4</sub>NC<sub>10</sub>H<sub>7</sub>N(CH<sub>3</sub>)2CH<sub>2</sub>)2C<sub>6</sub>H<sub>4</sub>

Synonyms:(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

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Chemical Property of (CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

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Technology Process of (CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

There total 1 articles about (CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 623-24-5
1,4-bis(bromomethyl)benzene

: 608517-40-4
(1R,9R)-5-[5-(4-Methoxy-phenyl)-pyridin-2-yl]-10,10-dimethyl-6-aza-tricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-triene

: 608517-37-9
(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

Guidance literature:: (1R,9R)-5-[5-(4-Methoxy-phenyl)-pyridin-2-yl]-10,10-dimethyl-6-aza-tricyclo[7.1.1.0^2,7]undeca-2⁽⁷⁾,3,5-triene; With n-butyllithium; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -40 ℃; for 3h;

1,4-bis(bromomethyl)benzene; In tetrahydrofuran; hexane; at -40 - 20 ℃; Further stages.;
DOI:10.1039/b210625f

Reference yield: 99.0%

: 26042-63-7
silver(I) hexafluorophosphate

: 608517-37-9
(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

: 6Ag⁽¹⁺⁾*6(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄*6PF₆^(1-)=Ag₆((CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄)6(PF₆)6

Guidance literature:: In chloroform; acetonitrile; a soln. of AgPF6 in acetonitrile was added to a soln. of polypyridine inchloroform and acetonitrile, the mixt. was stirred for 10 min at room t emp.; the solvent was evapd. under reduced pressure; elem. anal.;
DOI:10.1016/j.ica.2004.07.028

Reference yield: 97.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 608517-37-9
(CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄

: 6Cu⁽¹⁺⁾*6(CH₃OC₆H₄C₅H₃NC₁₀H₇N(CH₃)2CH₂)2C₆H₄*6PF₆^(1-)=Cu₆((CH₃OC₆H₃C₅H₄NC₁₀H₇N(CH₃)2CH₂)2C₆H₄)6(PF₆)6

Guidance literature:: In chloroform; acetonitrile; a soln. of Cu-complex in acetonitrile was added to a soln. of polypyridine in chloroform and acetonitrile, the mixt. was stirred for 10 min at room temp.; the solvent was evapd. under reduced pressure;
DOI:10.1016/j.ica.2004.07.028