C₅₈H₈₉N₃O₂₂S

Base Information

Chemical Name:C₅₈H₈₉N₃O₂₂S
CAS No.:1642888-08-1
Molecular Formula:C₅₈H₈₉N₃O₂₂S
Molecular Weight:1212.42
Hs Code.:

C<sub>58</sub>H<sub>89</sub>N<sub>3</sub>O<sub>22</sub>S

Synonyms:C₅₈H₈₉N₃O₂₂S

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Chemical Property of C₅₈H₈₉N₃O₂₂S

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Technology Process of C₅₈H₈₉N₃O₂₂S

There total 7 articles about C₅₈H₈₉N₃O₂₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 929-59-9,892154-56-2
3,6-dioxa-1,8-diaminooctane

: 1642888-07-0
C₅₂H₇₅NO₂₁S

: 1642888-08-1
C₅₈H₈₉N₃O₂₂S

Guidance literature:: C₅₂H₇₅NO₂₁S; With O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

3,6-dioxa-1,8-diaminooctane; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1039/c4ra02516d

Reference yield:

: 623-69-8
1,3-dimethyl glycerol ether

: 1642888-08-1
C₅₈H₈₉N₃O₂₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium hydroxide / 16 h / 80 °C / Inert atmosphere

2.1: triphenylphosphine; triethylamine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3.1 h / 0 - 20 °C / Inert atmosphere

3.1: 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; 2,6-di-tert-butyl-pyridine / 24 h / 150 °C

4.1: N-ethyl-N,N-diisopropylamine; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.5 h / 20 °C

4.2: 0.5 h / 20 °C

With 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c4ra02516d

Reference yield:

: 929048-34-0
C₁₃H₂₈O₇

: 1642888-08-1
C₅₈H₈₉N₃O₂₂S

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; triethylamine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3.1 h / 0 - 20 °C / Inert atmosphere

2.1: 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; 2,6-di-tert-butyl-pyridine / 24 h / 150 °C

3.1: N-ethyl-N,N-diisopropylamine; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / N,N-dimethyl-formamide / 0.5 h / 20 °C

3.2: 0.5 h / 20 °C

With 2,6-di-tert-butyl-pyridine; di-isopropyl azodicarboxylate; O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 3-butyl-1-methyl-1H-imidazol-3-ium hexafluorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c4ra02516d