1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

Base Information

Chemical Name:1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene
CAS No.:144582-07-0
Molecular Formula:C₄₄H₅₄N₄O₆
Molecular Weight:734.936
Hs Code.:

Synonyms:1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

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Chemical Property of 1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

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Technology Process of 1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

There total 18 articles about 1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 144582-06-9
1,4-Bis<4-<2-((5-ethoxycarbonyl-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-(2-cyano-2-methoxycarbonylvinyl)-4-methylpyrrol-3-yl>butyl>benzene

: 144582-07-0
1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

Guidance literature:: With potassium hydroxide; In propan-1-ol; for 3h; Heating;

Reference yield:

: 19417-59-5
1,4-bis-(3-bromopropyl)-benzene

: 144582-07-0
1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

Guidance literature:: Multi-step reaction with 13 steps

1: ethanol

2: aq. KOH

3: SOCl₂ / 0.5 h / Heating

4: 57 percent / SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

5: 80 percent / B₂H₆ / tetrahydrofuran

6: 86 percent / PhCH₂ONa / Heating

7: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

8: dimethylformamide / 2 h / Heating

9: POCl₃ / CH₂Cl₂ / 0.5 h

10: 76.9 percent / cyclohexylamine / toluene / 2 h / Heating

11: SO₂Cl₂ / CH₂Cl₂ / 0.5 h / Ambient temperature

12: 92 percent / acetic acid / 0.5 h / 70 °C

13: 93 percent / aq. KOH / propan-1-ol / 3 h / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen; tin(IV) chloride; cyclohexylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;

Reference yield:

: 19417-58-4
[1,4-phenylene]-bis(3-hydroxypropane)

: 144582-07-0
1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene

Guidance literature:: Multi-step reaction with 14 steps

1: HBr

2: ethanol

3: aq. KOH

4: SOCl₂ / 0.5 h / Heating

5: 57 percent / SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

6: 80 percent / B₂H₆ / tetrahydrofuran

7: 86 percent / PhCH₂ONa / Heating

8: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

9: dimethylformamide / 2 h / Heating

10: POCl₃ / CH₂Cl₂ / 0.5 h

11: 76.9 percent / cyclohexylamine / toluene / 2 h / Heating

12: SO₂Cl₂ / CH₂Cl₂ / 0.5 h / Ambient temperature

13: 92 percent / acetic acid / 0.5 h / 70 °C

14: 93 percent / aq. KOH / propan-1-ol / 3 h / Heating

With potassium hydroxide; thionyl chloride; sulfuryl dichloride; hydrogen bromide; hydrogen; tin(IV) chloride; cyclohexylamine; sodium phenyl-methanolate; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; toluene;