5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide

Base Information

• Chemical Name: 5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide
• CAS No.: 139547-50-5
• Molecular Formula: C₄₂H₂₉N₇O
• Molecular Weight: 647.739

Synonyms:5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide

Chemical Property of 5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide

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Technology Process of 5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide

There total 4 articles about 5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

pyridine-4-carbaldehyde (872-85-5) + pyrrole (109-97-7,30604-81-0) + 4-methoxy-benzaldehyde (123-11-5) → 5-(4-methoxyphenyl)-10,15,20-tris(4-pyridyl)porphyrin (139547-50-5)

Guidance literature:

With propionic acid; for 3h; Reflux;

DOI:10.1002/chem.201304344

Reference yield: 5.0%

pyridine-4-carbaldehyde (872-85-5) + pyrrole (109-97-7,30604-81-0) + 4-methoxy-benzaldehyde (123-11-5) → 5-(4-methoxyphenyl)-10,15,20-tri(N-methylpyridinium-4-yl)porphyrin triiodide (139547-50-5)

Guidance literature:

In propionic acid; for 0.833333h; Reflux;

DOI:10.1016/j.jphotochem.2020.112524

Reference yield: 3.0%

pyridine-4-carbaldehyde (872-85-5) + pyrrole (109-97-7,30604-81-0) + 4-methoxy-benzaldehyde (123-11-5) → 5,10-bis(4-methoxyphenyl)-15,20-bis(4-pyridyl)porphyrin + 5,15-bis(4-methoxyphenyl)-10,20-bis(4-pyridyl)porphyrin + 5-(4-methoxyphenyl)-10,15,20-tris(4-pyridyl)porphyrin (139547-50-5)

Guidance literature:

With propionic acid; at 110 ℃; for 4h; Reflux;

DOI:10.1142/S1088424619501438

upstream raw materials:

pyridine-4-carbaldehyde

pyrrole

4-methoxy-benzaldehyde

Downstream raw materials:

5-(4-hydroxyphenyl)-10,15,20-tris(pyridin-4-yl)porphyrin

5-(4-hydroxyphenyl)-10,15,20-tri-(4-pyridyl)-21,23H-porphyrin

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