2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan

Base Information

• Chemical Name: 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan
• CAS No.: 103212-29-9
• Molecular Formula: C₂₆H₂₈O₃
• Molecular Weight: 388.507
• Mol file: 103212-29-9.mol

Synonyms:2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan

Chemical Property of 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan

There total 3 articles about 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

1-(2,4,6-trimethylphenyl)-1,3-butanedione (6450-57-3) → 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan (103212-29-9) + C26H28O3

Guidance literature:

With carbon dioxide; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; caesium carbonate; In N,N-dimethyl-formamide; at 25 ℃; for 15h; under 3800.26 Torr; Irradiation;

DOI:10.1039/d1sc06403g

Reference yield:

2,5-dimethylfuran-3,4-dicarboxylic acid (14597-13-8) → 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan (103212-29-9)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride

2: aluminium chloride; carbon disulfide

With carbon disulfide; aluminium trichloride; thionyl chloride;

DOI:10.1021/jo01086a013

Reference yield:

2,5-dimethyl-furan-3,4-dicarbonyl chloride (51783-63-2) + 1,3,5-trimethyl-benzene (108-67-8) → 2,5-Dimethyl-3,4-bis-(2,4,6-trimethyl-benzoyl)-furan (103212-29-9)

Guidance literature:

With carbon disulfide; aluminium trichloride;

DOI:10.1021/jo01086a013

upstream raw materials:

2,5-dimethyl-furan-3,4-dicarbonyl chloride

1,3,5-trimethyl-benzene

2,5-dimethylfuran-3,4-dicarboxylic acid

1-(2,4,6-trimethylphenyl)-1,3-butanedione

Refernces