2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

Base Information

Chemical Name:2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene
CAS No.:219492-86-1
Molecular Formula:C₁₈H₂₁N₅O₃
Molecular Weight:355.396
Hs Code.:

Synonyms:2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

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Chemical Property of 2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

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Technology Process of 2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

There total 4 articles about 2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3320-86-3
2-nitrophenyl isocyanate

: 166954-15-0
C-(3,4,5,6-tetrahydro-2H-[1,4']bipyridinyl-4-yl)-methylamine

: 219492-86-1
2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

Guidance literature:: In tetrahydrofuran; chloroform;
DOI:10.1021/jm990625b

Reference yield:

: 121912-29-6
1-(pyridin-4-yl)piperidine-4-carboxylic acid ethyl ester

: 219492-86-1
2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: LiAlH₄

2.1: phthalimide; diethylazodicarboxylate; Ph₃P / tetrahydrofuran

2.2: hydrazine monohydrate / ethanol / 70 °C

3.1: CHCl₃; tetrahydrofuran

With lithium aluminium tetrahydride; phthalimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; chloroform; 1.1: Reduction / 2.1: Mitsunobu reaction / 2.2: Decomposition / 3.1: Condensation;
DOI:10.1021/jm990625b

Reference yield:

: 130658-67-2
4-hydroxymethyl-1-(pyridin-4-yl)piperidine

: 219492-86-1
2-[1-(pyridin-4-yl)piperidin-4-ylmethylaminocarbonyl]amino-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: phthalimide; diethylazodicarboxylate; Ph₃P / tetrahydrofuran

1.2: hydrazine monohydrate / ethanol / 70 °C

2.1: CHCl₃; tetrahydrofuran

With phthalimide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; chloroform; 1.1: Mitsunobu reaction / 1.2: Decomposition / 2.1: Condensation;
DOI:10.1021/jm990625b