[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

Base Information

Chemical Name:[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid
CAS No.:454466-05-8
Molecular Formula:C₄₁H₄₄N₄O₁₇
Molecular Weight:864.817
Hs Code.:

Synonyms:[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

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Chemical Property of [(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

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Technology Process of [(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

There total 2 articles about [(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 65055-19-8
2,3-bis(acetyloxy)benzoyl chloride

: 112013-58-8
{2-[bis-(2-amino-ethyl)-amino]-ethylamino}-acetic acid

: 454466-05-8
[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

Guidance literature:: In sodium hydrogencarbonate; at 0 - 5 ℃; for 1h;

Reference yield:

: 4097-89-6
2,2',2''-triaminotriethylamine

: 454466-05-8
[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂ / Pd/C / methanol / 20 °C

2: 50 percent / aq. NaHCO₃ / 1 h / 0 - 5 °C

With hydrogen; palladium on activated charcoal; In methanol; sodium hydrogencarbonate;

Reference yield: 61.0%

: 69-53-4
ampicillin

: 454466-05-8
[(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid

: (2S,5R,6R)-6-((R)-2-{2-[(2-{Bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetylamino}-2-phenyl-acetylamino)-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid

Guidance literature:: [(2-{bis-[2-(2,3-diacetoxy-benzoylamino)-ethyl]-amino}-ethyl)-(2,3-diacetoxy-benzoyl)-amino]-acetic acid; With 4-methyl-morpholine; methyl chloroformate; In tetrahydrofuran; at -10 ℃; for 1h;

ampicillin; With triethylamine; In tetrahydrofuran;