phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Base Information

Chemical Name:phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside
CAS No.:1160811-79-9
Molecular Formula:C₄₇H₄₆O₉
Molecular Weight:754.877
Hs Code.:

Synonyms:phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Suppliers and Price of phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

There total 1 articles about phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1160811-76-6
1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

: 74-95-3
1,1-dibromomethane

: 1160811-79-9
phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc; In tetrahydrofuran; dichloromethane; at 62 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.200802179

Reference yield: 80.0%

: 1160811-79-9
phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

: 1160811-81-3
phenyl 6a-C-(2b,6b-anhydro-5b,7b-O-benzylidene-1,3,4-trideoxy-α-D-glycero-D-manno-heptit-3-en-1-yl)-2,3,4-tri-O-benzyl-6-deoxy-6-oxo-α-D-mannopyranoside

Guidance literature:: With anion-exchange resin IRA-400; In 5,5-dimethyl-1,3-cyclohexadiene; at 220 ℃; for 0.333333h; under 2120.36 Torr; Microwave irradiation;
DOI:10.1002/chem.200802179

Reference yield: 56.0%

: 1160811-79-9
phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

: 1160811-81-3
phenyl 6a-C-(2b,6b-anhydro-5b,7b-O-benzylidene-1,3,4-trideoxy-α-D-glycero-D-manno-heptit-3-en-1-yl)-2,3,4-tri-O-benzyl-6-deoxy-6-oxo-α-D-mannopyranoside

: 1160811-80-2
phenyl 2,3,4-tri-O-benzyl-6-[4-(buta-1'Z,3'E-dienyl)-2-phenyl-1,3-dioxan-5-olyl]-6-deoxy-6-oxo-α-D-mannopyranoside

Guidance literature:: With anion-exchange resin IRA-400; In 5,5-dimethyl-1,3-cyclohexadiene; at 220 ℃; for 0.333333h; Microwave irradiation;
DOI:10.1002/chem.200802179