1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

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Chemical Name:1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate
CAS No.:1160811-76-6
Molecular Formula:C₄₆H₄₄O₁₀
Molecular Weight:756.849
Hs Code.:

Synonyms:1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

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Chemical Property of 1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

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Technology Process of 1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

There total 1 articles about 1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 63598-38-9,167074-37-5
1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-ribo-hex-1-enopyranose

: 1160811-73-3
phenyl 2,3,4-tri-O-benzyl-α-D-mannuronic acid

: 1160811-76-6
1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.200802179

Reference yield: 64.0%

: 1160811-76-6
1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl-(phenyl 2,3,4-tri-O-benzyl-α-D-mannopyranoside) uronate

: 74-95-3
1,1-dibromomethane

: 1160811-79-9
phenyl 6-O-(1b,5b-anhydro-4b,6b-O-benzylidene-2b-deoxy-D-ribo-hex-1-en-3b-yl)-7-deoxy-2,3,4-tri-O-benzyl-α-D-gluco-hept-6-enopyranoside

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc; In tetrahydrofuran; dichloromethane; at 62 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.200802179