3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

Base Information

Chemical Name:3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride
CAS No.:484046-58-4
Molecular Formula:C₃₄H₆₁ClO₁₅
Molecular Weight:745.302
Hs Code.:

Synonyms:3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

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Chemical Property of 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

Chemical Property:

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Technology Process of 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

There total 4 articles about 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 484046-57-3
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl alcohol

: 484046-58-4
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; for 1h;
DOI:10.1002/1099-0690(200208)2002:15<2587::AID-EJOC2587>3.0.CO;2-2

Reference yield:

: 484046-55-1
methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

: 484046-58-4
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

2: 100 percent / thionyl chloride / CH₂Cl₂ / 1 h

With lithium aluminium tetrahydride; thionyl chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/1099-0690(200208)2002:15<2587::AID-EJOC2587>3.0.CO;2-2

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 484046-58-4
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / water; tetrahydrofuran / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 70 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

4: thionyl chloride

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; sodium hydroxide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1002/anie.202006877