diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

Base Information

Chemical Name:diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate
CAS No.:941579-67-5
Molecular Formula:C₃₈H₇₁O₁₈P
Molecular Weight:846.945
Hs Code.:

Synonyms:diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

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Chemical Property of diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

Chemical Property:

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Technology Process of diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

There total 3 articles about diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 484046-58-4
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl chloride

: 122-52-1
triethyl phosphite

: 941579-67-5
diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

Guidance literature:: at 160 ℃; for 8h;
DOI:10.1039/b103966k

Reference yield:

: 484046-57-3
3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl alcohol

: 941579-67-5
diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 13.42 mmol / SOCl₂; DMF / CH₂Cl₂ / 1 h

2: 8 h / 160 °C

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1039/b103966k

Reference yield:

: 484046-55-1
methyl 3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzoate

: 941579-67-5
diethyl (3,4,5-tris(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)benzyl)phosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / Heating

2: 13.42 mmol / SOCl₂; DMF / CH₂Cl₂ / 1 h

3: 8 h / 160 °C

With lithium aluminium tetrahydride; thionyl chloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b103966k