[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4]

Base Information

• Chemical Name: [Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4]
• CAS No.: 89557-60-8
• Molecular Formula: C₁₃H₃₀FeO₆P₃*C₂₄H₂₀B
• Molecular Weight: 750.38

Synonyms:[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4]

Chemical Property of [Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4]

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Technology Process of [Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4]

There total 1 articles about [Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)2(P(CH₃)3)2(P(OCH₃)3)(COCH₃)][B(C₆H₅)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

[Fe(CO)3(P(CH3)3)2CH3](1+)*B(C6H5)4(1-)=[Fe(CO)3(P(CH3)3)2CH3][B(C6H5)4] (82660-92-2,60703-93-7) + phosphorous acid trimethyl ester (121-45-9) → [Fe(CO)2(P(CH3)3)2(P(OCH3)3)(COCH3)](1+)*B(C6H5)4(1-)=[Fe(CO)2(P(CH3)3)2(P(OCH3)3)(COCH3)][B(C6H5)4] (89557-60-8)

Guidance literature:

In dichloromethane; under N2, to soln. of complex equiv. of ligand added at room temp.; pptd. by hexane, filtered off; elem. anal.;

Reference yield: 90.0%

[Fe(CO)2(P(CH3)3)2(P(OCH3)3)(COCH3)](1+)*B(C6H5)4(1-)=[Fe(CO)2(P(CH3)3)2(P(OCH3)3)(COCH3)][B(C6H5)4] (89557-60-8) → FeCH3(CO)2(P(OCH3)3)(P(CH3)3)2(1+)*B(C6H5)4(1-)=(FeCH3(CO)2(P(OCH3)3)(P(CH3)3)2)(B(C6H5)4) (89557-49-3)

Guidance literature:

With nitrogen; In dichloromethane; soln. of complex left in N2 stream for 8 h at room temp.; pptd. with hexane; elem. anal.;

upstream raw materials:

[Fe(CO)3(P(CH₃)3)2CH₃]⁽¹⁺⁾*B(C₆H₅)4^(1-)=[Fe(CO)3(P(CH₃)3)2CH₃][B(C₆H₅)4]

phosphorous acid trimethyl ester

Downstream raw materials:

FeCH₃(CO)2(P(OCH₃)3)(P(CH₃)3)2⁽¹⁺⁾*B(C₆H₅)4^(1-)=(FeCH₃(CO)2(P(OCH₃)3)(P(CH₃)3)2)(B(C₆H₅)4)

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