C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾
CAS No.:1416992-48-7
Molecular Formula:C₂₅H₃₅N₄O₉S*Na
Molecular Weight:590.63
Hs Code.:

C<sub>25</sub>H<sub>35</sub>N<sub>4</sub>O<sub>9</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

Synonyms:C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

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Chemical Property of C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

There total 7 articles about C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1385183-82-3
benzyl ((S)-1-(((S)-4-(cyclopropylamino)-3,4-dioxo-1-(2-oxopyrrolidin-3-yl)butan-2-yl)amino)-4-methyl-1-oxopentan-2-yl)-carbamate

: 1416992-48-7
C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

Guidance literature:: With water; sodium hydrogensulfite; In ethanol; ethyl acetate; at 40 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.11.026

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 1416992-48-7
C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 9 steps

1: 1,4-dioxane

2: triethylamine

3: lithium hydroxide; water / tetrahydrofuran

4: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

5: lithium borohydride / tetrahydrofuran

6: Dess-Martin periodane / dichloromethane

7: acetic acid

8: Dess-Martin periodane / dichloromethane

9: sodium hydrogensulfite; water / ethanol; ethyl acetate / 2 h / 40 °C

With lithium borohydride; water; benzotriazol-1-ol; Dess-Martin periodane; sodium hydrogensulfite; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.11.026

Reference yield:

: 51021-87-5
N-benzyloxycarbonyl-L-leucine methyl ester

: 1416992-48-7
C₂₅H₃₅N₄O₉S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

1: lithium hydroxide; water / tetrahydrofuran

2: benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

3: lithium borohydride / tetrahydrofuran

4: Dess-Martin periodane / dichloromethane

5: acetic acid

6: Dess-Martin periodane / dichloromethane

7: sodium hydrogensulfite; water / ethanol; ethyl acetate / 2 h / 40 °C

With lithium borohydride; water; benzotriazol-1-ol; Dess-Martin periodane; sodium hydrogensulfite; acetic acid; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.11.026