Technology Process of N-tritylsulfenyl imine of acetone
There total 3 articles about N-tritylsulfenyl imine of acetone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridinium p-toluenesulfonate; magnesium sulfate;
In
dichloromethane;
for 2h;
Ambient temperature;
DOI:10.1021/jo00168a031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 88 percent / Sulfuryl chloride / toluene; diethyl ether / 2 h / 0 °C
2: 78 percent / 29 percent NH4OH/H2O / CH2Cl2 / 0 °C
3: 98 percent / Pridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO4 / CH2Cl2 / 2 h / Ambient temperature
With
ammonium hydroxide; sulfuryl dichloride; water; pyridinium p-toluenesulfonate; magnesium sulfate;
In
diethyl ether; dichloromethane; toluene;
DOI:10.1021/jo00168a031
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 78 percent / 29 percent NH4OH/H2O / CH2Cl2 / 0 °C
2: 98 percent / Pridinium p-toluenesulfonate, (PPTS)/anhydr. MgSO4 / CH2Cl2 / 2 h / Ambient temperature
With
ammonium hydroxide; water; pyridinium p-toluenesulfonate; magnesium sulfate;
In
dichloromethane;
DOI:10.1021/jo00168a031
