(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

Base Information

Chemical Name:(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran
CAS No.:161458-58-8
Molecular Formula:C₁₃H₁₆O₅S
Molecular Weight:284.333
Hs Code.:

Synonyms:(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

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Technology Process of (2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

There total 6 articles about (2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1007594-85-5
C₁₃H₁₅IO₅S

: 161458-58-8
(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

Guidance literature:: C₁₃H₁₅IO₅S; With methyllithium lithium chloride complex; In tetrahydrofuran; diethyl ether; at -20 ℃; for 1.66667h;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Product distribution / selectivity;

Reference yield: 72.0%

: 1001547-72-3
(3S,3aS,6S,6aS)-6-bromohexahydrofuro[3,2-b]furan-3-yI 4-methylbenzenesulfonate

: 161458-58-8
(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

Guidance literature:: With ammonium chloride; zinc; In isopropyl alcohol; for 16h; Product distribution / selectivity;

Reference yield:

: 54522-28-0,66966-12-9,67890-26-0,76793-35-6,107740-09-0
(3R,3aS,6S,6aS)-hexahydrofuro[3,2-b]furan-3,6-diyl bis(4-methylbenzenesulfonate)

: 161458-58-8
(2S,1'S)-(-)-2-<2-Hydroxy-1-(p-toluenesulfonyloxy)ethyl>-2,5-dihydrofuran

Guidance literature:: With methyllithium; sodium iodide; Yield given. Multistep reaction; 1.) acetone, 110 deg C, 20 h, 2.) THF, Et₂O, -78 deg C, 15 min;
DOI:10.1021/jo00106a030