(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

Base Information

Chemical Name:(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane
CAS No.:1334723-07-7
Molecular Formula:C₁₅H₂₂O₆
Molecular Weight:298.336
Hs Code.:

Synonyms:(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

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Chemical Property of (2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

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Technology Process of (2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

There total 3 articles about (2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 127943-23-1
1-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-4-hydroxybenzene

: 70987-78-9,6746-81-2
(S)-Glycidyl tosylate

: 1334723-07-7
(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

Guidance literature:: 1-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-4-hydroxybenzene; With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 2.33333h; Inert atmosphere;

(S)-Glycidyl tosylate; In N,N-dimethyl-formamide; at 50 ℃; for 96h; Inert atmosphere;
DOI:10.1007/s10847-010-9782-8

Reference yield:

: 77544-68-4
8-tosyloxy-3,6-dioxaoctanol

: 1334723-07-7
(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere; Heating

1.2: Inert atmosphere; Heating

2.1: palladium on activated charcoal; hydrogen / methanol; dichloromethane / 48 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 2.33 h / 50 °C / Inert atmosphere

3.2: 96 h / 50 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s10847-010-9782-8

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 1334723-07-7
(2S)-(+)-3-phenoxy-4-[2-(2-(2-hydroxyethoxy)ethoxy)ethoxy]-1,2-epoxypropane

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere; Heating

1.2: Inert atmosphere; Heating

2.1: palladium on activated charcoal; hydrogen / methanol; dichloromethane / 48 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / N,N-dimethyl-formamide / 2.33 h / 50 °C / Inert atmosphere

3.2: 96 h / 50 °C / Inert atmosphere

With palladium on activated charcoal; hydrogen; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s10847-010-9782-8