tetraethylene glycol monobenzyl mono-12-bromododecyl ether

Base Information

Chemical Name:tetraethylene glycol monobenzyl mono-12-bromododecyl ether
CAS No.:1424097-93-7
Molecular Formula:C₂₇H₄₇BrO₅
Molecular Weight:531.571
Hs Code.:

Synonyms:tetraethylene glycol monobenzyl mono-12-bromododecyl ether

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Chemical Property of tetraethylene glycol monobenzyl mono-12-bromododecyl ether

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Technology Process of tetraethylene glycol monobenzyl mono-12-bromododecyl ether

There total 3 articles about tetraethylene glycol monobenzyl mono-12-bromododecyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 3344-70-5
1,12-dibromododecane

: 86259-87-2,1201808-31-2
1-phenyl-2,5,8,11-tetraoxatridecan-13-ol

: 1424097-93-7
tetraethylene glycol monobenzyl mono-12-bromododecyl ether

Guidance literature:: 1-phenyl-2,5,8,11-tetraoxatridecan-13-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h;

1,12-dibromododecane; In tetrahydrofuran; mineral oil;
DOI:10.1039/c3cc38949a

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1424097-93-7
tetraethylene glycol monobenzyl mono-12-bromododecyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

1.2: 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

With sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c3cc38949a

Reference yield:

: 100-39-0
benzyl bromide

: 1424097-93-7
tetraethylene glycol monobenzyl mono-12-bromododecyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

1.2: 20 °C

2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 0 °C

With sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c3cc38949a