Technology Process of C21H21NO2
There total 13 articles about C21H21NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran; chlorobenzene;
Heating;
DOI:10.1039/c39890000186
- Guidance literature:
-
Multi-step reaction with 13 steps
1: 97 percent / H(1+)
2: 76 percent / TiCl4 / CH2Cl2 / 0 °C
3: 78 percent / NaH / dimethylformamide
4: 1.) m-chloroperbenzoic acid; 2.) HCl, H2O / 1.) CH2Cl2; 2.) CH3OH
5: 71 percent / K2CO3 / acetone
6: 1.) LiAlH4; 2.) BaMnO4 / 1.) ether; 2.) CH2Cl2
7: sodium methoxide / methanol / -15 °C
8: xylene / Heating
9: 99 percent / LiAlH4 / diethyl ether
10: 69 percent / BaMnO4 / CH2Cl2
11: 80 percent / NaH / dimethylformamide
12: 77 percent / methanol
13: 84 percent / NaH / chlorobenzene; tetrahydrofuran / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; barium permanganate; water; sodium methylate; hydrogen cation; titanium tetrachloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; acetone; xylene;
DOI:10.1039/c39890000186
- Guidance literature:
-
Multi-step reaction with 12 steps
1: 76 percent / TiCl4 / CH2Cl2 / 0 °C
2: 78 percent / NaH / dimethylformamide
3: 1.) m-chloroperbenzoic acid; 2.) HCl, H2O / 1.) CH2Cl2; 2.) CH3OH
4: 71 percent / K2CO3 / acetone
5: 1.) LiAlH4; 2.) BaMnO4 / 1.) ether; 2.) CH2Cl2
6: sodium methoxide / methanol / -15 °C
7: xylene / Heating
8: 99 percent / LiAlH4 / diethyl ether
9: 69 percent / BaMnO4 / CH2Cl2
10: 80 percent / NaH / dimethylformamide
11: 77 percent / methanol
12: 84 percent / NaH / chlorobenzene; tetrahydrofuran / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; barium permanganate; water; sodium methylate; titanium tetrachloride; sodium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; chlorobenzene; acetone; xylene;
DOI:10.1039/c39890000186
