4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

Base Information

Chemical Name:4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide
CAS No.:117535-98-5
Molecular Formula:C₂₅H₃₄N₂O₃
Molecular Weight:410.557
Hs Code.:

Synonyms:4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

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Chemical Property of 4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

Chemical Property:

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Technology Process of 4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

There total 5 articles about 4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 117535-97-4
4-(3-chloropropoxy)-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

: 109-89-7
diethylamine

: 117535-98-5
4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 5h; pressure vessel;

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 117535-98-5
4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / K₂CO₃ / acetone / 40 h / Heating

2: 65 percent / 1N NaOH / 20 h / Ambient temperature

3: 75 percent / SOCl₂ / 6 h / Heating

4: 82 percent / sodium acetate / CHCl₃; H₂O / Ambient temperature; overnight

5: 72 percent / KI / dimethylformamide / 5 h / 100 °C / pressure vessel

With sodium hydroxide; thionyl chloride; sodium acetate; potassium carbonate; potassium iodide; In chloroform; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 69182-93-0
4-(3-chloropropoxy)phenylacetic acid

: 117535-98-5
4-<3-(N,N-diethylamino)propoxy>-N-<3-(4-phenyl-2-oxobutyl)>phenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / SOCl₂ / 6 h / Heating

2: 82 percent / sodium acetate / CHCl₃; H₂O / Ambient temperature; overnight

3: 72 percent / KI / dimethylformamide / 5 h / 100 °C / pressure vessel

With thionyl chloride; sodium acetate; potassium iodide; In chloroform; water; N,N-dimethyl-formamide;