N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

Base Information

Chemical Name:N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester
CAS No.:148150-67-8
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

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Chemical Property of N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

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Technology Process of N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

There total 3 articles about N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3143-02-0
3-hydroxymethyl-3-methyloxethane

: 73724-45-5
N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine

: 148150-67-8
N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

: (S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-3-hydroxy-propionic acid (S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-2-(3-methyl-oxetan-3-ylmethoxycarbonyl)-ethyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 3h;

Reference yield:

: 99314-44-0
(3-methyloxetan-3-yl)methyl 4-methylbenzenesulfonate

: 148150-67-8
N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaBr / acetone / 30 h / Heating

2: 1.) Cs₂CO₃ / 1.) H₂O, 20 min, 2.) DMF, room temperature, 24 h

With caesium carbonate; sodium bromide; In acetone;
DOI:10.1021/jo972294l

Reference yield:

: 78385-26-9
3-bromomethyl-3-methyloxetane

: 73724-45-5
N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine

: 148150-67-8
N-(9-fluorenylmethyloxycarbonyl)-L-serine 3-methyl-3-(hydroxymethyl)oxetane ester

Guidance literature:: With caesium carbonate; Yield given. Multistep reaction; 1.) H₂O, 20 min, 2.) DMF, room temperature, 24 h;
DOI:10.1021/jo972294l