tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane
CAS No.:289618-05-9
Molecular Formula:C₆₅H₄₅N₃O₂Si
Molecular Weight:928.177
Hs Code.:

Synonyms:tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

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Chemical Property of tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

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Technology Process of tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

There total 2 articles about tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18162-48-6
tert-butyldimethylsilyl chloride

: 289618-01-5
(2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethanol

: 289618-05-9
tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ja0009119

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 289618-01-5
(2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethanol

: 289618-05-9
tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

Guidance literature:: With 2,6-di-tert-butyl-pyridine; In benzene; at 20 ℃; for 1h;
DOI:10.1021/ja0009119

Reference yield:

: 2923-28-6
silver trifluoromethanesulfonate

: 289618-05-9
tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane

: tert-butyl((2,4,6-tris(4-((4-cyanophenyl)ethynyl)phenylethynyl)phenoxy)ethoxy)dimethylsilane*AgCF₃SO₃

Guidance literature:: In benzene; to soln. of ligand added soln. of SiCF3SO3, heatet from room temp. to 98°C at 0.5 degree/min, held at 98°C for 70 min, then slowly cooled to room temp. at 0.1°C/min;
DOI:10.1021/ja0009119