2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

Base Information

Chemical Name:2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt
CAS No.:1061696-48-7
Molecular Formula:C₁₃H₁₄NO₁₀S*K
Molecular Weight:415.419
Hs Code.:

Synonyms:2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

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Chemical Property of 2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

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Technology Process of 2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

There total 5 articles about 2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1061696-45-4
5-nitrooxyvaleric acid 4-nitrophenylester potassium salt

: 108-24-7
acetic anhydride

: 1061696-48-7
2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

Guidance literature:: With dmap; In acetone; at 0 - 25 ℃; for 6h;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1061696-48-7
2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 8.5 h / 0 - 20 °C

2.1: silver nitrate / acetonitrile / 30 h / 60 °C

3.1: sulfuric acid; hydroquinone / n-heptane; water / 1 h / 0 - 60 °C / pH 5 - 5.5

3.2: 8 h / 25 - 30 °C

4.1: dmap / acetone / 6 h / 0 - 25 °C

With dmap; sulfuric acid; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; In n-heptane; dichloromethane; water; acetone; acetonitrile;

Reference yield:

: 2067-33-6
5-bromopentanoic acid

: 1061696-48-7
2-(acetyloxy)-5-{[5-(nitrooxy)pentanoyl]oxy}benzenesulfonic acid potassium salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 8.5 h / 0 - 20 °C

2.1: silver nitrate / acetonitrile / 30 h / 60 °C

3.1: sulfuric acid; hydroquinone / n-heptane; water / 1 h / 0 - 60 °C / pH 5 - 5.5

3.2: 8 h / 25 - 30 °C

4.1: dmap / acetone / 6 h / 0 - 25 °C

With dmap; sulfuric acid; silver nitrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; In n-heptane; dichloromethane; water; acetone; acetonitrile;