C₃₇H₆₅NO₄Si₂

Base Information

Chemical Name:C₃₇H₆₅NO₄Si₂
CAS No.:1246937-52-9
Molecular Formula:C₃₇H₆₅NO₄Si₂
Molecular Weight:644.098
Hs Code.:

C<sub>37</sub>H<sub>65</sub>NO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₇H₆₅NO₄Si₂

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Chemical Property of C₃₇H₆₅NO₄Si₂

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Technology Process of C₃₇H₆₅NO₄Si₂

There total 7 articles about C₃₇H₆₅NO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1246937-70-1
C₁₉H₂₅NO₂

: 1246937-51-8
(S)-4,6-bis(tert-butyldimethylsilyloxy)hex-2-yne

: C₃₁H₄₉NO₃Si

: 1246937-52-9
C₃₇H₆₅NO₄Si₂

Guidance literature:: With triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride; In toluene; at -78 - -30 ℃; Inert atmosphere;
DOI:10.1002/anie.201002220

Reference yield:

: 73842-99-6
3-tert-butyldimethylsilyloxy-1-propanol

: C₃₁H₄₉NO₃Si

: 1246937-52-9
C₃₇H₆₅NO₄Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / Inert atmosphere

2.1: (-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine / toluene / 0.08 h

2.2: 17 h

3.1: 2,6-dimethylpyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

4.1: triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride / toluene / -78 - -30 °C

With 2,6-dimethylpyridine; triisopropoxytitanium(IV) chloride; (-)-N-methylephedrine; sulfur trioxide pyridine complex; zinc trifluoromethanesulfonate; cyclopentylmagnesium chloride; dimethyl sulfoxide; triethylamine; In dichloromethane; toluene; 1.1: Parikh-Doering oxidation / 4.1: Negishi coupling reaction;
DOI:10.1021/jo202119p

Reference yield:

: 89922-82-7
3-(tert-butyldimethylsilanyloxy)propionaldehyde

: C₃₁H₄₉NO₃Si

: 1246937-52-9
C₃₇H₆₅NO₄Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: (-)-N-methylephedrine; zinc trifluoromethanesulfonate; triethylamine / toluene / 0.08 h

1.2: 17 h

2.1: 2,6-dimethylpyridine / dichloromethane / 4 h / 20 °C / Inert atmosphere

3.1: triisopropoxytitanium(IV) chloride; cyclopentylmagnesium chloride / toluene / -78 - -30 °C

With 2,6-dimethylpyridine; triisopropoxytitanium(IV) chloride; (-)-N-methylephedrine; zinc trifluoromethanesulfonate; cyclopentylmagnesium chloride; triethylamine; In dichloromethane; toluene; 3.1: Negishi coupling reaction;
DOI:10.1021/jo202119p