N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

Base Information

Chemical Name:N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester
CAS No.:110920-78-0
Molecular Formula:C₃₁H₃₀N₂O₁₂
Molecular Weight:622.585
Hs Code.:

N<sup>3</sup>,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

Synonyms:N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

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Chemical Property of N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

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Technology Process of N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

There total 3 articles about N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110920-77-9
N³,5'-O-dibenzoyl-5-bromo-2',3'-O-isopropylideneuridine

: 108-59-8
malonic acid dimethyl ester

: 110920-78-0
N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; for 15h; Ambient temperature;

Reference yield:

: 98-88-4
benzoyl chloride

: 110920-78-0
N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94.9 percent / dimethylaminopyridine, triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 95 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / 15 h / Ambient temperature

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 54503-61-6
2',3'-O-isopropylidene-5-bromouridine

: 110920-78-0
N³,5'-O-dibenzoyl-2',3'-O-isopropylideneuridine-5-malonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94.9 percent / dimethylaminopyridine, triethylamine / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 95 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / tetrahydrofuran / 15 h / Ambient temperature

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; dichloromethane;