5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin

Base Information

• Chemical Name: 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin
• CAS No.: 124362-39-6
• Molecular Formula: C₅₈H₅₆N₆O₁₀
• Molecular Weight: 997.117
• Mol file: 124362-39-6.mol

Synonyms:5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin

Chemical Property of 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin

There total 2 articles about 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.3%

pyridine-4-carbaldehyde (872-85-5) + pyrrole (109-97-7,30604-81-0) → 5-(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,15,20-tri(4-pyridyl)porphyrin (124384-07-2) + 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin (124362-39-6) + 5,10-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-15,20-di(4-pyridyl)porphyrin (124362-40-9) + 5,10,15,20-tetra(4-pyridyl)-21H,23H-porphine (16834-13-2)

Guidance literature:

With benzo-15-crown-5-ether; In propionic acid; Further byproducts given; 1.) reflux, 1 h, 2.) room temperature, 2 days;

Reference yield:

pyridine-4-carbaldehyde (872-85-5) + pyrrole (109-97-7,30604-81-0) + benzo-15-crown-5-ether (60835-73-6) → 5-(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,15,20-tri(4-pyridyl)porphyrin (124384-07-2) + 5,15-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-10,20-di(4-pyridyl)porphyrin (124362-39-6) + 5,10-di(2,3-benzo-1,4,7,10,13-pentaoxa-2-cyclopentadecen-4'-yl)-15,20-di(4-pyridyl)porphyrin (124362-40-9) + 5,10,15,20-tetra(4-pyridyl)-21H,23H-porphine (16834-13-2)

Guidance literature:

In propionic acid; Further byproducts given; 1.) reflux, 1 h, 2.) room temperature, 2 days;

upstream raw materials:

pyridine-4-carbaldehyde

pyrrole

benzo-15-crown-5-ether