N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide

Base Information

Chemical Name:N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide
CAS No.:119825-39-7
Molecular Formula:C₃₉H₅₉ClN₂O₁₁
Molecular Weight:767.357
Hs Code.:

Synonyms:N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide

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Chemical Property of N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide

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Technology Process of N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide

There total 6 articles about N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 64-18-6
formic acid

: 630-18-2
tert-butyl isocyanide

: 104-88-1
4-chlorobenzaldehyde

: 108342-87-6,120029-97-2,120030-03-7
N-[2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl]amine

: 112022-98-7,119825-39-7
2,2-Dimethyl-propionic acid (2R,3R,4S,5R,6R)-2-{[(S)-tert-butylcarbamoyl-(4-chloro-phenyl)-methyl]-formyl-amino}-4,5-bis-(2,2-dimethyl-propionyloxy)-6-(2,2-dimethyl-propionyloxymethyl)-tetrahydro-pyran-3-yl ester

: 112022-98-7,119825-39-7
2,2-Dimethyl-propionic acid (2R,3R,4S,5R,6R)-2-{[(R)-tert-butylcarbamoyl-(4-chloro-phenyl)-methyl]-formyl-amino}-4,5-bis-(2,2-dimethyl-propionyloxy)-6-(2,2-dimethyl-propionyloxymethyl)-tetrahydro-pyran-3-yl ester

Guidance literature:: With zinc chloride diethyl ether; In tetrahydrofuran; at -25 ℃; for 24h;
DOI:10.1021/ja00210a084

Reference yield: 92.0%

: 64-18-6
formic acid

: 630-18-2
tert-butyl isocyanide

: 104-88-1
4-chlorobenzaldehyde

: 108342-87-6,120029-97-2,120030-03-7
N-[2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl]amine

: 112022-98-7,119825-39-7
2,2-Dimethyl-propionic acid (2R,3R,4S,5R,6R)-2-{[(S)-tert-butylcarbamoyl-(4-chloro-phenyl)-methyl]-formyl-amino}-4,5-bis-(2,2-dimethyl-propionyloxy)-6-(2,2-dimethyl-propionyloxymethyl)-tetrahydro-pyran-3-yl ester

: 112022-98-7,119825-39-7
2,2-Dimethyl-propionic acid (2R,3R,4S,5R,6R)-2-{[(R)-tert-butylcarbamoyl-(4-chloro-phenyl)-methyl]-formyl-amino}-4,5-bis-(2,2-dimethyl-propionyloxy)-6-(2,2-dimethyl-propionyloxymethyl)-tetrahydro-pyran-3-yl ester

Guidance literature:: With zinc chloride diethyl ether; In tetrahydrofuran; at -25 ℃; for 24h;
DOI:10.1021/ja00210a084

Reference yield: 92.0%

: 64-18-6
formic acid

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 104-88-1
4-chlorobenzaldehyde

: 108342-87-6
tetra-O-pivaloyl-β-D-galactopyranosylamine

: 119825-39-7
N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(S)-p-chloro-phenylglycine-N'-tert-butyl-amide

: 112022-98-7
N-formyl-N-(2,3,4,6-tetra-O-pivaloyl-β-D-galactopyranosyl)-(R)-p-chloro-phenylglycine-N'-tert-butyl-amide

Guidance literature:: With zinc chloride diethyl ether; In tetrahydrofuran; dichloromethane; at -25 ℃; for 24h; Yields of byproduct given;
DOI:10.1016/S0040-4020(01)86054-3