5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

Base Information

Chemical Name:5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride
CAS No.:1356708-17-2
Molecular Formula:C₂₉H₃₃NO₂*ClH
Molecular Weight:464.047
Hs Code.:

Synonyms:5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

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Chemical Property of 5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

Chemical Property:

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Technology Process of 5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

There total 5 articles about 5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 1356708-21-8
5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl

: 1356708-17-2
5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

Guidance literature:: With hydrogenchloride; In water; Product distribution / selectivity;

Reference yield:

: 528-43-8
Magnolol

: 1356708-17-2
5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; 18-crown-6 ether / acetone / 17 h

2: triphenylphosphine; diethylazodicarboxylate / toluene / 17 h / 0 - 80 °C

3: hydrogenchloride / dichloromethane / 0.17 h

With hydrogenchloride; 18-crown-6 ether; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In dichloromethane; acetone; toluene;

Reference yield:

: 18776-12-0,125712-82-5
3-chloro-1-phenyl-propan-1-ol

: 1356708-17-2
5,5'-diallyl-2-methoxy-2'-[3-(methylamino)-1-phenylpropoxy]biphenyl hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus tribromide / diethyl ether / 2 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C

2.2: 60 h / 0 - 20 °C

3.1: water; tetrahydrofuran / 120 h / 20 °C

4.1: hydrogenchloride / dichloromethane / 0.17 h

With hydrogenchloride; phosphorus tribromide; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;