Orotic acid benzylidene hydrazide

Base Information

• Chemical Name: Orotic acid benzylidene hydrazide
• CAS No.: 115547-71-2
• Molecular Formula: C₁₂H₁₀N₄O₃
• Molecular Weight: 258.236
• Mol file: 115547-71-2.mol

Synonyms:Orotic acid benzylidene hydrazide

Chemical Property of Orotic acid benzylidene hydrazide

Chemical Property:

Purity/Quality:

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Technology Process of Orotic acid benzylidene hydrazide

There total 1 articles about Orotic acid benzylidene hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Orotic acid hydrazide (26409-12-1,26696-56-0) + benzaldehyde (100-52-7) → Orotic acid benzylidene hydrazide (115547-71-2)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 4h;

DOI:10.1007/BF00768247

Reference yield: 75.0%

Orotic acid benzylidene hydrazide (115547-71-2) → 2,6-Dioxo-1,2,3,6-tetrahydro-pyrimidine-4-carboxylic acid N'-benzyl-hydrazide (115547-65-4)

Guidance literature:

With sodium tetrahydroborate; buffer solution (Na₂B₄O₇/NaOH); at 15 - 20 ℃; for 26h; pH 10.02;

DOI:10.1007/BF00768247

upstream raw materials:

Orotic acid hydrazide

benzaldehyde

Downstream raw materials:

2,6-Dioxo-1,2,3,6-tetrahydro-pyrimidine-4-carboxylic acid N'-benzyl-hydrazide