(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

Base Information

Chemical Name:(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone
CAS No.:146896-37-9
Molecular Formula:C₁₉H₁₈O₂Se
Molecular Weight:357.311
Hs Code.:

Synonyms:(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

Chemical Property:

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Technology Process of (2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

There total 4 articles about (2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1666-13-3
diphenyl diselenide

: 10225-38-4
1-phenyl-2-(2-propenyl)-1,3-butanedione

: 146896-37-9
(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

: 146896-35-7
3-acetyl-4,5-dihydro-2-phenyl-5-<(phenylseleno)methyl>furan

Guidance literature:: With iodine pentoxide; In acetonitrile; at 20 ℃; for 0.166667h;
DOI:10.1039/d1ob02196f

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 10225-38-4
1-phenyl-2-(2-propenyl)-1,3-butanedione

: 146896-37-9
(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

Guidance literature:: In tetrahydrofuran; at 20 ℃;
DOI:10.3184/030823408X320629

Reference yield:

: 93-91-4
1-phenylbutan-1,3-dione

: 146896-37-9
(2-methyl-5-((phenylselanyl)methyl)-4,5-dihydrofuran-3-yl)(phenyl)methanone

: 146896-35-7
3-acetyl-4,5-dihydro-2-phenyl-5-<(phenylseleno)methyl>furan

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

1.2: 0 - 20 °C

2.1: tetrabutylammonium tetrafluoroborate; acetic acid / acetonitrile / 0 °C / Inert atmosphere; Electrochemical reaction; Green chemistry

With tetrabutylammonium tetrafluoroborate; sodium hydride; acetic acid; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c9gc02665g