1-Phenyl-2-allyl-1,3-butanedione

Base Information

• Chemical Name: 1-Phenyl-2-allyl-1,3-butanedione
• CAS No.: 10225-38-4
• Molecular Formula: C13H14O2
• Molecular Weight: 202.253
• Hs Code.: 2914399090
• Mol file: 10225-38-4.mol

Synonyms:2-allyl-1-phenyl-1,3-butanedione;2-Allyl-1-phenylbutandione-1,3;2-allyl-1-phenylbutane-1,3-dione;1-phenyl-2-(2-propenyl)-1,3-butanedione;3-Allyl-benzoylaceton;2-Acetoxy-1-phenyl-pent-4-en-1-on;1,3-Butanedione,1-phenyl-2-(2-propenyl);1,3-Butanedione,2-allyl-1-phenyl;1-Phenyl-2-allyl-1,3-butanedione;

Chemical Property of 1-Phenyl-2-allyl-1,3-butanedione

Chemical Property:

• PSA: 34.14000
• LogP: 2.65060

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenyl-2-allyl-1,3-butanedione

There total 9 articles about 1-Phenyl-2-allyl-1,3-butanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

allyl bromide (106-95-6) + 1-phenylbutan-1,3-dione (93-91-4) → 1-phenyl-2-(2-propenyl)-1,3-butanedione (10225-38-4)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide;

DOI:10.1021/ja00533a018

Reference yield: 84.0%

allyl methyl carbonate (35466-83-2) + 1-phenylbutan-1,3-dione (93-91-4) → 1-phenyl-2-(2-propenyl)-1,3-butanedione (10225-38-4)

Guidance literature:

Pd-montmorillonite; In ethanol; at 80 ℃; for 25h;

DOI:10.1002/anie.200604644

Reference yield: 81.0%

Allyl acetate (591-87-7) + 1-phenylbutan-1,3-dione (93-91-4) → 1-phenyl-2-(2-propenyl)-1,3-butanedione (10225-38-4)

Guidance literature:

With trisodium tris(3-sulfophenyl)phosphine; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-3-methylimidazolium tetrafluoroborate; palladium diacetate; In water; for 0.15h; microwave irradiation;

DOI:10.1016/j.tetlet.2005.04.002

upstream raw materials:

allyl bromide

1-phenylbutan-1,3-dione

3-chloroprop-1-ene

5-Hexen-2-one

Downstream raw materials:

(2,5-dimethylfuran-3-yl)(phenyl)methanone

4-allyl-1-(4-methoxyphenyl)-3-methyl-5-phenyl-1H-pyrazole

4-allyl-1-(4-methoxyphenyl)-5-methyl-3-phenyl-1H-pyrazole

4-allyl-1,3-dimethyl-5-phenyl-1H-pyrazole