N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

Base Information

Chemical Name:N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine
CAS No.:1417366-39-2
Molecular Formula:C₁₆H₉Br₂Cl₂N₃
Molecular Weight:473.982
Hs Code.:

Synonyms:N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

Suppliers and Price of N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

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Technology Process of N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

There total 1 articles about N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1417366-35-8
6,8-dibromo-4-chloroquinoline-3-carbaldehyde

: 1073-70-7
4-chlorophenylhydrazine hydrochloride

: 1417366-39-2
N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

Guidance literature:: With triethylamine; In ethanol; at 60 ℃; for 12h;
DOI:10.1016/j.tet.2012.10.103

Reference yield: 89.0%

: 1417366-39-2
N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

: 1417366-43-8
6,8-dibromo-1-(4-chlorophenyl)-1H-pyrazolo[4,3-c]quinoline

Guidance literature:: With potassium hydroxide; In ethanol; at 80 ℃; for 3h;
DOI:10.1016/j.tet.2012.10.103

Reference yield:

: 1417366-39-2
N-[(6,8-dibromo-4-chloroquinolin-3-yl)methylene]-2-(4-chlorophenyl)hydrazine

: 1417366-53-0
1-(4-chlorophenyl)-6,8-diphenyl-1H-pyrazolo[4,3-c]quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 3 h / 80 °C

2: bis-triphenylphosphine-palladium(II) chloride; tricyclohexylphosphine; potassium carbonate / N,N-dimethyl-formamide; water / 3 h / 80 - 90 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; potassium hydroxide; tricyclohexylphosphine; In ethanol; water; N,N-dimethyl-formamide; 2: |Suzuki-Miyaura Coupling;
DOI:10.1016/j.tet.2012.10.103