methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide

Base Information

Chemical Name:methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide
CAS No.:1088410-49-4
Molecular Formula:C₃₀H₄₀N₄O₆S₂
Molecular Weight:616.803
Hs Code.:

Synonyms:methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide

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Chemical Property of methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide

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Technology Process of methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide

There total 1 articles about methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 64-18-6
formic acid

: 1088409-50-0
methyl (7S)-6-N-((2′S,4′R)-4′-(cyclopropylmethyl)piperidine-2′-carbonyl)-7-deoxy-7-(4-(pyrimidin-5-yl)phenylthio)-α-thiolincosaminide

: 1088410-49-4
methyl 6-N-((2S,4R)-4-cyclopropylmethyl-1-formylpipecoloyl)-7-deoxy-7-epi-7-(4-(pyrimidin-5-yl)phenylthio)-1-thio-α-lincosamide

Guidance literature:: formic acid; With acetic anhydride; at 60 ℃; for 1h;

methyl (7S)-6-N-((2′S,4′R)-4′-(cyclopropylmethyl)piperidine-2′-carbonyl)-7-deoxy-7-(4-(pyrimidin-5-yl)phenylthio)-α-thiolincosaminide; In methanol; at 60 ℃; for 16h;

With ammonia; In chloroform; water; acetone;