(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

Base Information

Chemical Name:(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone
CAS No.:1246523-61-4
Molecular Formula:C₅₀H₄₈N₂O₇
Molecular Weight:788.94
Hs Code.:

Synonyms:(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

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Chemical Property of (7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

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Technology Process of (7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

There total 42 articles about (7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: [5-bromo-7-(tert-butoxy)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl](4-methoxyphenyl)methanone

: 124-41-4
sodium methylate

: 1246523-61-4
(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

Guidance literature:: With copper(l) iodide; In methanol; N,N-dimethyl-formamide; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201703279

Reference yield: 62.0%

: 1246523-60-3
(4-(2-azido-3-(tert-butoxy)phenyl)-6-methoxy-1-(4-methoxyphenethyl)-3,7-bis(4-methoxyphenyl)-1H-indol-2-yl)(4-methoxyphenyl)methanone

: 1246523-61-4
(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

Guidance literature:: In 1,4-dioxane; at 180 ℃; for 0.5h; Flow reactor;
DOI:10.1002/anie.201500067

Reference yield:

: 14425-64-0
4-methoxyphenethyl bromide

: 1246523-61-4
(7-(tert-butoxy)-5-methoxy-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-2-yl)(4-methoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 2 h

2.1: zinc(II) chloride / diethyl ether / 0 °C

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / 1,4-dioxane / 3 h / Reflux

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium hydroxide / 1,4-dioxane; water / 1.5 h / 20 °C

5.1: 1,2-dichloro-benzene / 0.67 h / Reflux; Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; potassium hydroxide; sodium hydroxide; zinc(II) chloride; In 1,4-dioxane; diethyl ether; water; N,N-dimethyl-formamide; 1,2-dichloro-benzene; 4.1: Suzuki-Miyaura coupling;
DOI:10.1002/asia.201000544