1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

Base Information

Chemical Name:1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide
CAS No.:1613039-73-8
Molecular Formula:C₁₆H₁₄N₄O
Molecular Weight:278.313
Hs Code.:

Synonyms:1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

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Chemical Property of 1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

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Technology Process of 1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

There total 3 articles about 1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 34296-51-0
1-phenyl-1,2,3-triazole-4-carbaldehyde

: 29601-98-7
N-benzylhydroxylamine hydrochloride

: 1613039-73-8
1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

Guidance literature:: With sodium hydrogencarbonate; In ethanol; at 60 ℃; Reagent/catalyst;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 103755-58-4
(1-phenyl-1H-1,2,3-triazole-4-yl)methanol

: 1613039-73-8
1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: Jones reagent / acetone / 0.58 h / 0 °C

2: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; sodium hydrogencarbonate; In ethanol; acetone;
DOI:10.1016/j.ejmech.2014.04.052

Reference yield:

: 622-37-7
Phenyl azide

: 1613039-73-8
1-phenyl-N-((1-phenyl-1H-1,2,3-triazol-4-yl)methylene)methanamine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: copper diacetate / water; tert-butyl alcohol / 18 h / 20 °C / Inert atmosphere

2: Jones reagent / acetone / 0.58 h / 0 °C

3: sodium hydrogencarbonate / ethanol / 60 °C

With Jones reagent; copper diacetate; sodium hydrogencarbonate; In ethanol; water; acetone; tert-butyl alcohol;
DOI:10.1016/j.ejmech.2014.04.052