chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)

Base Information

Chemical Name:chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)
CAS No.:53470-05-6
Molecular Formula:C₅₆H₅₂ClFeN₄O₁₂
Molecular Weight:1064.35
Hs Code.:

Synonyms:chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)

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Chemical Property of chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)

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Technology Process of chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)

There total 4 articles about chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.4%

: meso-tetrakis-(2,4,6-methoxyphenyl)porphyrin

: 7439-89-6
iron

: 53470-05-6
chloro[tetrakis(2,4,6-trimethoxyphenyl)porphinato]iron(III)

Guidance literature:: With sodium chloride; In chloroform; acetic acid; refluxing iron powder and glacial acetic acid, 24h; addn. of porphyrin and NaCl to CHCl3; stirring, 15 min; addn. to iron soln.; refluxing, 2h;reducing volume; addn. of water; sonication; filtration; drying solid (vac.); chromy. (acid alumina, CHCl3); evapn.;addn. of heptane; evapn. up to pptn.; refigerating overnight; elem. anal.;

Reference yield:

: 53470-07-8
[meso-tetrakis(2,4,6-trimethoxyphenyl)porphyrin]iron(II)

: 1665-00-5
dichloromethane-d2

: 53470-05-6
5,10,15,20-tetrakis(2',4',6'-trimethoxyphenyl)porphyrinatoiron(III) chloride

: 81245-22-9
{(meso-tetrakis(2,4,6-trimethoxyphenyl)porphyrinato)iron(III)OH}

Guidance literature:: With oxygen; In dichloromethane-d2; O2 was added to a soln. of Fe-complex in CD2Cl2 at -80°C, warmedto room temp.; monitored by NMR (1)H;
DOI:10.1021/ja00386a027

Reference yield:

: meso-tetrakis-(2,4,6-methoxyphenyl)porphyrin

: iron(II) chloride

: 53470-05-6
5,10,15,20-tetrakis(2',4',6'-trimethoxyphenyl)porphyrinatoiron(III) chloride

Guidance literature:: With HCl; In N,N-dimethyl-formamide; treating of a refluxing soln. of the porphyrin in DMF with FeCl2, extn. (CHCl3), shaking with concd. HCl in air; sepn. of the CHCl3 layer, purifn. by chromy.;
DOI:10.1016/S0020-1693(00)80883-X