DIETHYL 6-HYDRAZINO-2-OXO-1,2-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE

Base Information

• Chemical Name: DIETHYL 6-HYDRAZINO-2-OXO-1,2-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE
• CAS No.: 146255-50-7
• Molecular Formula: C₁₁H₁₅N₃O₅
• Molecular Weight: 269.257
• Mol file: 146255-50-7.mol

Synonyms:diethyl 6-hydrazino-1,2-dihydro-2-oxo-3,5-pyridinedicarboxylate

Chemical Property of DIETHYL 6-HYDRAZINO-2-OXO-1,2-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE

Chemical Property:

Purity/Quality:

Diethyl 6-hydrazino-2-oxo-1,2-dihydro-3,5-pyridinedicarboxylate ^*data from reagent suppliers

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Technology Process of DIETHYL 6-HYDRAZINO-2-OXO-1,2-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE

There total 1 articles about DIETHYL 6-HYDRAZINO-2-OXO-1,2-DIHYDRO-3,5-PYRIDINEDICARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

diethyl 1,2-dihydro-6-ethoxy-2-oxo-3,5-pyridinedicarboxylate (93475-38-8) → diethyl 6-hydrazino-1,2-dihydro-2-oxo-3,5-pyridinedicarboxylate (146255-50-7)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Heating;

Reference yield: 95.0%

benzoyl chloride (98-88-4) + diethyl 6-hydrazino-1,2-dihydro-2-oxo-3,5-pyridinedicarboxylate (146255-50-7) → 6-(N'-Benzoyl-hydrazino)-2-oxo-1,2-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

Guidance literature:

With pyridine; at 0 ℃; for 3h;

Reference yield: 65.0%

diethyl 6-hydrazino-1,2-dihydro-2-oxo-3,5-pyridinedicarboxylate (146255-50-7) + phenylacetyl chloride (103-80-0) → 2-Oxo-6-(N'-phenylacetyl-hydrazino)-1,2-dihydro-pyridine-3,5-dicarboxylic acid diethyl ester

Guidance literature:

With pyridine; at 0 ℃; for 3h;

upstream raw materials:

diethyl 1,2-dihydro-6-ethoxy-2-oxo-3,5-pyridinedicarboxylate

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