CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl

Base Information

• Chemical Name: CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl
• CAS No.: 206008-10-8
• Molecular Formula: C₁₉H₃₀Cl₂N₂O₅S₄Sn₃
• Molecular Weight: 921.758
• Mol file: 206008-10-8.mol

Synonyms:CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl

Chemical Property of CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl

There total 1 articles about CH₃OSn(CH₃)2S(NSO₂C₆H₄Cl)Sn(CH₃)2SSn(CH₃)2NHSO₂C₆H₄Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane (16892-64-1) + N-chloro-p-chlorobenzenesulfonamide sodium salt (30066-82-1) → CH3OSn(CH3)2S(NSO2C6H4Cl)Sn(CH3)2SSn(CH3)2NHSO2C6H4Cl (206008-10-8) + sulfur (7704-34-9) + sodium chloride (7647-14-5)

Guidance literature:

In methanol; soln. of N-compd. addn. to soln. of Sn compd. (vacuum, stirring), heating (50°C, 30 min); mixture cooling (ice bath), ppt. filtration off and extracting with water to remove NaCl and with acetone to remove S, alcoholic filtrate vacuumevapn., residue treating with diethyl ether, soln. decanting and vacuum evapn.; elem. anal.;

Reference yield:

CH3OSn(CH3)2S(NSO2C6H4Cl)Sn(CH3)2SSn(CH3)2NHSO2C6H4Cl (206008-10-8) + water (7732-18-5) → 4-Chlorobenzenesulfonamide (98-64-6) + hydroxydimethyltin sulfite (206008-12-0) + hydroxydimethyltin sulfate (206008-11-9) + 2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane (16892-64-1)

Guidance literature:

In diethyl ether; byproducts: CH3OH; treating with moist ether, sepn. of NaCl and S, filtrate evapn. in vacuum; ppt. washing (hot water), Sn-compd. remaining on the filtration paper, N-compd. pptn. on cooling (5°C), residue insoluble in ether were Sn-containing sulfite and Sn-containing sulfate; IR spectroscopy;

upstream raw materials:

2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane

N-chloro-p-chlorobenzenesulfonamide sodium salt

Downstream raw materials:

4-Chlorobenzenesulfonamide

hydroxydimethyltin sulfite

hydroxydimethyltin sulfate

2,2,4,4,6,6-hexamethyl-1,3,5,2,4,6-trithiatristanninane

Refernces