4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Base Information

Chemical Name:4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde
CAS No.:1355159-89-5
Molecular Formula:C₂₄H₂₀N₂O₃
Molecular Weight:384.434
Hs Code.:

Synonyms:4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

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Chemical Property of 4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

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Technology Process of 4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

There total 8 articles about 4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1141473-63-3
(4-{5-[2-(methoxymethyl)-2'-methylbiphenyl-4-yl]-1,2,4-oxadiazol-3-yl}phenyl)methanol

: 1355159-89-5
4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: With manganese(IV) oxide; In 1,4-dioxane; at 70 ℃;

Reference yield:

: 874-89-5
4-Cyanobenzyl alcohol

: 1355159-89-5
4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: hydroxylamine / ethanol; water / 16 h / 74 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 18 h / 20 °C / Microwave irradiation

3: manganese(IV) oxide / 1,4-dioxane / 70 °C

With manganese(IV) oxide; hydroxylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In 1,4-dioxane; ethanol; water; acetonitrile;

Reference yield:

: 142031-67-2
methyl 4-bromo-3-(bromomethyl)benzoate

: 1355159-89-5
4-(5-(2-(methoxymethyl)-2'-methylbiphenyl-4-yl)-1,2,4-oxadiazol-3-yl)benzaldehyde

Guidance literature:: Multi-step reaction with 5 steps

1.1: 96 h / Reflux

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; water / Inert atmosphere; Reflux

3.1: sodium hydroxide / ethanol / 1 h / 60 °C

3.2: pH 2

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / acetonitrile / 18 h / 20 °C / Microwave irradiation

5.1: manganese(IV) oxide / 1,4-dioxane / 70 °C

With manganese(IV) oxide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; ethanol; water; toluene; acetonitrile;