(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

Base Information

Chemical Name:(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium
CAS No.:1286180-86-6
Molecular Formula:C₁₀H₁₀BrO₆S*Na
Molecular Weight:361.146
Hs Code.:

Synonyms:(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

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Chemical Property of (4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

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Technology Process of (4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

There total 2 articles about (4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286179-94-9
methyl 3-bromo-6-bromomethyl-2-methoxybenzoate

: 1286180-86-6
(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

Guidance literature:: With sodium sulfite; In ethanol; water; for 2h; Reflux;

Reference yield:

: methyl 3-bromo-2-methoxy-6-methylbenzoate

: 1286180-86-6
(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

Guidance literature:: Multi-step reaction with 2 steps

1: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 3 h / illuminated with a 500W tungsten filament lamp

2: sodium sulfite / ethanol; water / 2 h / Reflux

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sodium sulfite; 2,2'-azobis(isobutyronitrile); In ethanol; water; 1,2-dichloro-ethane;

Reference yield:

: 110-89-4
piperidine

: 1286180-86-6
(4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium

: 1286180-85-5
methyl 3-bromo-2-methoxy-6-(piperidin-1-ylsulphonylmethyl)benzoate

Guidance literature:: (4-bromo-3-methoxy-2-methoxycarbonylphenyl)-methanesulphonic acid sodium; With thionyl chloride; In dichloromethane; at 50 ℃; for 2h;

piperidine; In dichloromethane; at 20 ℃; for 4h;