2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

Base Information

Chemical Name:2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole
CAS No.:110589-04-3
Molecular Formula:C₃₄H₄₈N₂O₅
Molecular Weight:564.766
Hs Code.:

Synonyms:2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

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Chemical Property of 2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

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Technology Process of 2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

There total 10 articles about 2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 110569-83-0
2,6-bis<5-<5-(ethoxycarbonyl)-4-methypyrrol-3-yl>-1-pentenyl>-4-methylanisole

: 110589-04-3
2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

Guidance literature:: With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; for 24h; Ambient temperature;
DOI:10.1021/jo00233a011

Reference yield:

: 6327-85-1
2,6-bis(hydroxymethyl)-4-methyl-anisole

: 110589-04-3
2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DMSO/(COCl)2, 2.) Et₃N / 1.) methylene chloride, -78 deg C, 15 min, 2.) methylene chloride, from -78 deg C to RT

2: 47.1 percent / K₂CO₃ / dioxane / 45 h / Heating

3: 91.7 percent / H₂, Et₃N / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature

With oxalyl dichloride; hydrogen; potassium carbonate; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jo00233a011

Reference yield:

: 71128-83-1
2-methoxy-5-methyl-1,3-benzenedicarboxaldehyde

: 110589-04-3
2,6-bis<5-<5-(ethoxycarbonyl)-4-methylpyrrol-3-yl>-pentyl>-4-methylanisole

Guidance literature:: Multi-step reaction with 2 steps

1: 47.1 percent / K₂CO₃ / dioxane / 45 h / Heating

2: 91.7 percent / H₂, Et₃N / 10percent Pd/C / tetrahydrofuran / 24 h / Ambient temperature

With hydrogen; potassium carbonate; triethylamine; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/jo00233a011