3,4-dideoxyhexaric acid

Base Information

• Chemical Name: 3,4-dideoxyhexaric acid
• CAS No.: 13544-77-9
• Molecular Formula: C6H10 O6
• Molecular Weight: 178.142
• Mol file: 13544-77-9.mol

Synonyms:Hexanedioic acid,2,5-dihydroxy- (7CI); 2,5-Dihydroxyadipic acid; 3,4-Dideoxyhexaric acid; NSC509382

Chemical Property of 3,4-dideoxyhexaric acid

Chemical Property:

• Vapor Pressure: 1.4E-10mmHg at 25°C
• Boiling Point: 464.5°Cat760mmHg
• Flash Point: 248.9°C
• Density: 1.582g/cm³

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,4-dideoxyhexaric acid

There total 3 articles about 3,4-dideoxyhexaric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl meso-2,5-diiodohexanedioate (165334-67-8) → (2E,4E)-2,4-hexadienedioic acid (3588-17-8) + 2,5-dihydroxyadipic acid (13544-77-9)

Guidance literature:

higher-melting α.α'-diiodo-adipic acid diethyl ester;

Reference yield:

diethyl 2,5-dibromoadipate (869-10-3) → (2E,4E)-2,4-hexadienedioic acid (3588-17-8) + 2,5-dihydroxyadipic acid (13544-77-9)

Guidance literature:

higher-melting α.α'-dibromo-adipic acid diethyl ester;

Reference yield:

1,2,5,6-hexanetetrol (20221-50-5,24211-51-6,122923-46-0,5581-21-5) → 2-hydroxyglutaric acid (2889-31-8,636-67-9) + 2,5-dihydroxyadipic acid (13544-77-9)

Guidance literature:

With sodium hydroxide; In water; at 60 - 150 ℃; for 16h;

upstream raw materials:

diethyl 2,5-dibromoadipate

diethyl meso-2,5-diiodohexanedioate

1,2,5,6-hexanetetrol

Downstream raw materials:

butanedial

cis-tetrahydrofuran-2,5-dicarboxylic acid

succinic acid