(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

Base Information

Chemical Name:(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine
CAS No.:1379012-39-1
Molecular Formula:C₂₀H₁₈BrNOS
Molecular Weight:400.339
Hs Code.:

Synonyms:(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

Chemical Property:

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Technology Process of (1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

There total 3 articles about (1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1379012-29-9
C₂₀H₁₈BrNS

: 1379012-39-1
(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

Guidance literature:: With sodium tungstate (VI) dihydrate; dihydrogen peroxide; acetic acid; In water; at 20 ℃; for 0.0333333h;
DOI:10.1039/c2cc31907a

Reference yield:

: 23190-16-1
(1R,2S)-2-Amino-1,2-diphenylethanol

: 1379012-39-1
(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

Guidance literature:: Multi-step reaction with 3 steps

1: di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine / tetrahydrofuran / 20 h / 20 °C

2: methanol / 8 h / Reflux

3: sodium tungstate (VI) dihydrate; dihydrogen peroxide; acetic acid / water / 0.03 h / 20 °C

With sodium tungstate (VI) dihydrate; di-isopropyl azodicarboxylate; dihydrogen peroxide; acetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; water; 1: Mitsunobu reaction;
DOI:10.1039/c2cc31907a

Reference yield:

: 1605-06-7,25125-72-8,26114-25-0,133522-23-3
(-)-(2S,3S)-2,3-diphenylaziridine

: 1379012-39-1
(1S,2R)-2-((R)-(4-bromophenyl)sulfinyl)-1,2-diphenylethanamine

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 8 h / Reflux

2: sodium tungstate (VI) dihydrate; dihydrogen peroxide; acetic acid / water / 0.03 h / 20 °C

With sodium tungstate (VI) dihydrate; dihydrogen peroxide; acetic acid; In methanol; water;
DOI:10.1039/c2cc31907a