trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

Base Information

Chemical Name:trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone
CAS No.:151592-94-8
Molecular Formula:C₁₈H₁₈N₂O₃
Molecular Weight:310.353
Hs Code.:

Synonyms:trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

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Technology Process of trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

There total 5 articles about trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 151490-63-0
trans-1-<(R)-(Methoxycarbonyl)(phenyl)methyl>-3-(S)-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentyl)-4(S)-phenyl-2-azetidinone

: 151592-94-8
trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; for 0.5h; Yield given;
DOI:10.1021/jo00119a009

Reference yield:

: 153924-62-0
N-benzylidenephenylglycine methyl ester

: 78605-23-9
ethyl 2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentane-1-acetate

: 151490-63-0
trans-1-<(R)-(Methoxycarbonyl)(phenyl)methyl>-3-(S)-(2,2,5,5-tetramethyl-1-aza-2,5-disilacyclopentyl)-4(S)-phenyl-2-azetidinone

: 151592-94-8
trans-3(S)-Amino-1-<(R)-(methoxycarbonyl)(phenyl)methyl>-4-(S)-phenyl-2-azetidinone

Guidance literature:: With zinc(II) chloride; lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) hexane, THF, -78 deg C, 15 min; 2.) -78 deg C to -30 deg C, 3 h; -30 deg C, 16 h;
DOI:10.1021/jo00119a009